![]() LowD 9 3 -temperature DMA data on other nylon 6Àclay nano-230 composites reported in show that it is centred around ¡50 C and that tan dD 9 4 begins to rise again when the temperature decreases below ✱5 C. ![]() In principle, brittleness and crack propagation at lower temperature could result in enhanced time-dependent deformationD 9 1, but we consider it more likely that the slight increase in creep depth at ¡10 C on D 9 2 nylon 6 and non-exfoliated nanocomposite is a consequence of being on the shoulder of the b relaxation peak of nylon 6. Decreasing the temperature below T g reduces the free volume.
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